Solid State Nuclear Magnetic Resonance (SS-NMR) @ Waterford Institute of Technology (WIT) PMBRC

Institution Waterford Institute of Technology (WIT) PMBRC
County Waterford
Technique Category Spectroscopy
Technique Solid State Nuclear Magnetic Resonance (SS-NMR)

Basic Capabilities

Broadband SS-NMR probe capable of measuring a broad range of nuclei including: 1H, 13C, 15N, 29Si, 27Al, 31P, 19F

Equipment

Equipment Make Joel
Equipment Model ECX 400 MHz

Advantages/Limitations

Advantage of Technique/Equipment

Can measure insoluble compounds and polymers; gain information on the solid state nature of the sample; reduced sample prep. required in some instances

Limitations of Technique/Equipment Experimental time can be somewhat longer than that of solution state NMR in some instances, depending on the sample.

Other Details

Containment Yes, high potency materials have been tested with this. Samples can be filled into the rotor in an isolator and brought to NMR lab
Turnaround Time Days
Report yes
Interpretation yes
Data on Analyst Experienced postdoctoral researcher
Indicative Price Depends on sample properties and time required for analysis. Price available on request

Industry Recommendation

Contact

Dr. Niall O'Reilly

Quality & Systems Supports

Quality Management System in Place

Internal quality management system (SOPs, logbooks)

Good Manufacturing Practice Status

Preventative Maintenance

PM contract in place

Accreditation

N/A

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